Nanocrystalline Fe/Zr alloys: Preparation by using mechanical alloying and mechanical milling processes

V. A.Peña Rodríguez; Medina M. Medina; Quispe Q. Marcatoma; Ch Rojas Ayala; C. V. Landauro; E. M. Baggio-Saitovitch; E. C. Passamani

doi:10.1007/s10751-011-0343-3

Nanocrystalline Fe/Zr alloys: Preparation by using mechanical alloying and mechanical milling processes

V. A.Peña Rodríguez, Medina M. Medina, Quispe Q. Marcatoma, Ch Rojas Ayala, C. V. Landauro, E. M. Baggio-Saitovitch, E. C. Passamani

Research output: Contribution to journal › Article › peer-review

1 Scopus citations

Abstract

Nanocrystalline Fe/Zr alloys have been prepared after milling for 9 h the mixture of elemental Fe and Zr powders or the arc-melting produced Fe₂Zr alloy by using mechanical alloying and mechanical milling techniques, respectively. X-ray and Mössbauer results of the Fe and Zr powders, mechanically alloyed, suggest that amorphous Fe₂Zr phase and α-Fe(Zr) nanograins have been produced with relative concentrations of 91% and 9%, respectively. Conversely, the results of the mechanically milled Fe₂Zr alloy indicate that nanograins of the Fe₂Zr alloy have been formed, surrounded by a magnetic inter-granular phase that are simultaneously dispersed in a paramagnetic amorphous phase.

Original language	English
Pages (from-to)	145-151
Number of pages	7
Journal	Hyperfine Interactions
Volume	202
Issue number	1-3
DOIs	https://doi.org/10.1007/s10751-011-0343-3
State	Published - Nov 2011
Externally published	Yes

Bibliographical note

Funding Information:
Acknowledgements The authors would like to acknowledge the financial support provided by CSI-UNMSM under Project No. 041301011, FAPERJ-Brazil (Cientista do Nosso Estado), FINEP, FAPES and Latin American Center of Physics.

Keywords

Fe Mössbauer spectroscopy
Mechanical alloying
Mechanical milling
Nanostructured materials

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10.1007/s10751-011-0343-3

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title = "Nanocrystalline Fe/Zr alloys: Preparation by using mechanical alloying and mechanical milling processes",

abstract = "Nanocrystalline Fe/Zr alloys have been prepared after milling for 9 h the mixture of elemental Fe and Zr powders or the arc-melting produced Fe2Zr alloy by using mechanical alloying and mechanical milling techniques, respectively. X-ray and M{\"o}ssbauer results of the Fe and Zr powders, mechanically alloyed, suggest that amorphous Fe2Zr phase and α-Fe(Zr) nanograins have been produced with relative concentrations of 91% and 9%, respectively. Conversely, the results of the mechanically milled Fe2Zr alloy indicate that nanograins of the Fe2Zr alloy have been formed, surrounded by a magnetic inter-granular phase that are simultaneously dispersed in a paramagnetic amorphous phase.",

keywords = "Fe M{\"o}ssbauer spectroscopy, Mechanical alloying, Mechanical milling, Nanostructured materials",

author = "Rodr{\'i}guez, {V. A.Pe{\~n}a} and Medina, {Medina M.} and Marcatoma, {Quispe Q.} and Ayala, {Ch Rojas} and Landauro, {C. V.} and Baggio-Saitovitch, {E. M.} and Passamani, {E. C.}",

note = "Funding Information: Acknowledgements The authors would like to acknowledge the financial support provided by CSI-UNMSM under Project No. 041301011, FAPERJ-Brazil (Cientista do Nosso Estado), FINEP, FAPES and Latin American Center of Physics.",

year = "2011",

month = nov,

doi = "10.1007/s10751-011-0343-3",

language = "Ingl{\'e}s",

volume = "202",

pages = "145--151",

journal = "Hyperfine Interactions",

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T2 - Preparation by using mechanical alloying and mechanical milling processes

AU - Rodríguez, V. A.Peña

AU - Medina, Medina M.

AU - Marcatoma, Quispe Q.

AU - Ayala, Ch Rojas

AU - Landauro, C. V.

AU - Baggio-Saitovitch, E. M.

AU - Passamani, E. C.

N1 - Funding Information: Acknowledgements The authors would like to acknowledge the financial support provided by CSI-UNMSM under Project No. 041301011, FAPERJ-Brazil (Cientista do Nosso Estado), FINEP, FAPES and Latin American Center of Physics.

PY - 2011/11

Y1 - 2011/11

N2 - Nanocrystalline Fe/Zr alloys have been prepared after milling for 9 h the mixture of elemental Fe and Zr powders or the arc-melting produced Fe2Zr alloy by using mechanical alloying and mechanical milling techniques, respectively. X-ray and Mössbauer results of the Fe and Zr powders, mechanically alloyed, suggest that amorphous Fe2Zr phase and α-Fe(Zr) nanograins have been produced with relative concentrations of 91% and 9%, respectively. Conversely, the results of the mechanically milled Fe2Zr alloy indicate that nanograins of the Fe2Zr alloy have been formed, surrounded by a magnetic inter-granular phase that are simultaneously dispersed in a paramagnetic amorphous phase.

AB - Nanocrystalline Fe/Zr alloys have been prepared after milling for 9 h the mixture of elemental Fe and Zr powders or the arc-melting produced Fe2Zr alloy by using mechanical alloying and mechanical milling techniques, respectively. X-ray and Mössbauer results of the Fe and Zr powders, mechanically alloyed, suggest that amorphous Fe2Zr phase and α-Fe(Zr) nanograins have been produced with relative concentrations of 91% and 9%, respectively. Conversely, the results of the mechanically milled Fe2Zr alloy indicate that nanograins of the Fe2Zr alloy have been formed, surrounded by a magnetic inter-granular phase that are simultaneously dispersed in a paramagnetic amorphous phase.

KW - Fe Mössbauer spectroscopy

KW - Mechanical alloying

KW - Mechanical milling

KW - Nanostructured materials

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DO - 10.1007/s10751-011-0343-3

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SN - 0304-3843

VL - 202

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EP - 151

JO - Hyperfine Interactions

JF - Hyperfine Interactions

IS - 1-3

ER -

Nanocrystalline Fe/Zr alloys: Preparation by using mechanical alloying and mechanical milling processes

Abstract

Bibliographical note

Keywords

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