Electrochemical Determination of Morin in Natural Food Using a Chitosan–Graphene Glassy Carbon Modified Electrode

Edgar Nagles; Monica Bello; John J. Hurtado

doi:10.3390/s22207780

Electrochemical Determination of Morin in Natural Food Using a Chitosan–Graphene Glassy Carbon Modified Electrode

Edgar Nagles, Monica Bello, John J. Hurtado

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Resumen

This report presents a new application for the chitosan–graphene glassy carbon electrode (Ch-G/GCE) system in the determination of the hydroxyflavonoid morin (MR), one of the flavonoids with the highest favorable activity for people, due to its natural properties by square-wave voltammetry (SWV). The anodic peak current for MR was observed at 0.50 V with an increase of 73% compared with the glassy carbon electrode unmodified. The surface areas of Ch-G/GCE, Ch/GCE and GCE evaluated by cyclic voltammetry were 0.140, 0.053 and 0.011 cm², respectively. Additionally, an increase greater than 100% compared to the electrode without modification was observed. The detection limit was 0.30 µmol/L for MR, and the relative standard deviations (RSDs) were 1.8% (n = 6). Possible interferences as quercetin, rutin, and applications in real samples were also evaluated with very acceptable results.

Idioma original	Inglés
Número de artículo	7780
Publicación	Sensors
Volumen	22
N.º	20
DOI	https://doi.org/10.3390/s22207780
Estado	Publicada - oct. 2022
Publicado de forma externa	Sí

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© 2022 by the authors.

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title = "Electrochemical Determination of Morin in Natural Food Using a Chitosan–Graphene Glassy Carbon Modified Electrode",

abstract = "This report presents a new application for the chitosan–graphene glassy carbon electrode (Ch-G/GCE) system in the determination of the hydroxyflavonoid morin (MR), one of the flavonoids with the highest favorable activity for people, due to its natural properties by square-wave voltammetry (SWV). The anodic peak current for MR was observed at 0.50 V with an increase of 73% compared with the glassy carbon electrode unmodified. The surface areas of Ch-G/GCE, Ch/GCE and GCE evaluated by cyclic voltammetry were 0.140, 0.053 and 0.011 cm2, respectively. Additionally, an increase greater than 100% compared to the electrode without modification was observed. The detection limit was 0.30 µmol/L for MR, and the relative standard deviations (RSDs) were 1.8% (n = 6). Possible interferences as quercetin, rutin, and applications in real samples were also evaluated with very acceptable results.",

keywords = "chitosan, glassy carbon, graphene, morin, square wave voltammetry",

author = "Edgar Nagles and Monica Bello and Hurtado, {John J.}",

note = "Publisher Copyright: {\textcopyright} 2022 by the authors.",

year = "2022",

month = oct,

doi = "10.3390/s22207780",

language = "Ingl{\'e}s",

volume = "22",

journal = "Sensors",

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TY - JOUR

T1 - Electrochemical Determination of Morin in Natural Food Using a Chitosan–Graphene Glassy Carbon Modified Electrode

AU - Nagles, Edgar

AU - Bello, Monica

AU - Hurtado, John J.

PY - 2022/10

Y1 - 2022/10

N2 - This report presents a new application for the chitosan–graphene glassy carbon electrode (Ch-G/GCE) system in the determination of the hydroxyflavonoid morin (MR), one of the flavonoids with the highest favorable activity for people, due to its natural properties by square-wave voltammetry (SWV). The anodic peak current for MR was observed at 0.50 V with an increase of 73% compared with the glassy carbon electrode unmodified. The surface areas of Ch-G/GCE, Ch/GCE and GCE evaluated by cyclic voltammetry were 0.140, 0.053 and 0.011 cm2, respectively. Additionally, an increase greater than 100% compared to the electrode without modification was observed. The detection limit was 0.30 µmol/L for MR, and the relative standard deviations (RSDs) were 1.8% (n = 6). Possible interferences as quercetin, rutin, and applications in real samples were also evaluated with very acceptable results.

AB - This report presents a new application for the chitosan–graphene glassy carbon electrode (Ch-G/GCE) system in the determination of the hydroxyflavonoid morin (MR), one of the flavonoids with the highest favorable activity for people, due to its natural properties by square-wave voltammetry (SWV). The anodic peak current for MR was observed at 0.50 V with an increase of 73% compared with the glassy carbon electrode unmodified. The surface areas of Ch-G/GCE, Ch/GCE and GCE evaluated by cyclic voltammetry were 0.140, 0.053 and 0.011 cm2, respectively. Additionally, an increase greater than 100% compared to the electrode without modification was observed. The detection limit was 0.30 µmol/L for MR, and the relative standard deviations (RSDs) were 1.8% (n = 6). Possible interferences as quercetin, rutin, and applications in real samples were also evaluated with very acceptable results.

KW - chitosan

KW - glassy carbon

KW - graphene

KW - morin

KW - square wave voltammetry

UR - http://www.scopus.com/inward/record.url?scp=85140582441&partnerID=8YFLogxK

U2 - 10.3390/s22207780

DO - 10.3390/s22207780

M3 - Artículo

AN - SCOPUS:85140582441

SN - 1424-8220

VL - 22

JO - Sensors

JF - Sensors

IS - 20

M1 - 7780

ER -

Electrochemical Determination of Morin in Natural Food Using a Chitosan–Graphene Glassy Carbon Modified Electrode

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