Magnetic Properties and Crystallization of the Fe75Si 15B10 Amorphous Alloy Prepared by Mechanical Alloying

J. Quispe Marcatoma; V. A. Peña Rodríguez; E. M. Baggio-Saitovitch

doi:10.1023/B:HYPE.0000003769.28718.19

Magnetic Properties and Crystallization of the Fe₇₅Si ₁₅B₁₀ Amorphous Alloy Prepared by Mechanical Alloying

J. Quispe Marcatoma, V. A. Peña Rodríguez, E. M. Baggio-Saitovitch

Producción científica: Contribución a una revista › Artículo › revisión exhaustiva

6 Citas (Scopus)

Resumen

The magnetic order and crystallization of the amorphous Fe ₇₅Si₁₅B₁₀ alloy prepared by mechanical alloying was studied in situ by ⁵⁷Fe Mössbauer spectroscopy. These measurements were carried out using a vacuum furnace, controlling the temperature in the absorber. From Mössbauer measurements the magnetic order temperature of the as-milled sample was estimated at about 675 K. In order to identify the crystalline phases formed during heating, Mössbauer measurements were analyzed together with X-ray diffraction analysis. Both results show the formation of several crystalline phases such as Fe ₅SiB₂, Fe₂B, Fe₃Si, α-Fe, Fe-B composite and a residual amorphous phase.

Idioma original	Inglés
Páginas (desde-hasta)	97-102
Número de páginas	6
Publicación	Hyperfine Interactions
Volumen	148-149
N.º	1-4
DOI	https://doi.org/10.1023/B:HYPE.0000003769.28718.19
Estado	Publicada - 2003
Publicado de forma externa	Sí

Acceder al documento

10.1023/B:HYPE.0000003769.28718.19

Otros archivos y enlaces

Enlace a la publicación en Scopus

Citar esto

@article{f6333575340948e4b2b949fdd2862ea3,

title = "Magnetic Properties and Crystallization of the Fe75Si 15B10 Amorphous Alloy Prepared by Mechanical Alloying",

abstract = "The magnetic order and crystallization of the amorphous Fe 75Si15B10 alloy prepared by mechanical alloying was studied in situ by 57Fe M{\"o}ssbauer spectroscopy. These measurements were carried out using a vacuum furnace, controlling the temperature in the absorber. From M{\"o}ssbauer measurements the magnetic order temperature of the as-milled sample was estimated at about 675 K. In order to identify the crystalline phases formed during heating, M{\"o}ssbauer measurements were analyzed together with X-ray diffraction analysis. Both results show the formation of several crystalline phases such as Fe 5SiB2, Fe2B, Fe3Si, α-Fe, Fe-B composite and a residual amorphous phase.",

keywords = "Mechanical alloying, Metallic alloys, M{\"o}ssbauer spectroscopy, Soft magnetic materials",

author = "{Quispe Marcatoma}, J. and {Pe{\~n}a Rodr{\'i}guez}, {V. A.} and Baggio-Saitovitch, {E. M.}",

year = "2003",

doi = "10.1023/B:HYPE.0000003769.28718.19",

language = "Ingl{\'e}s",

volume = "148-149",

pages = "97--102",

journal = "Hyperfine Interactions",

issn = "0304-3843",

publisher = "Springer Nature",

number = "1-4",

}

TY - JOUR

T1 - Magnetic Properties and Crystallization of the Fe75Si 15B10 Amorphous Alloy Prepared by Mechanical Alloying

AU - Quispe Marcatoma, J.

AU - Peña Rodríguez, V. A.

AU - Baggio-Saitovitch, E. M.

PY - 2003

Y1 - 2003

N2 - The magnetic order and crystallization of the amorphous Fe 75Si15B10 alloy prepared by mechanical alloying was studied in situ by 57Fe Mössbauer spectroscopy. These measurements were carried out using a vacuum furnace, controlling the temperature in the absorber. From Mössbauer measurements the magnetic order temperature of the as-milled sample was estimated at about 675 K. In order to identify the crystalline phases formed during heating, Mössbauer measurements were analyzed together with X-ray diffraction analysis. Both results show the formation of several crystalline phases such as Fe 5SiB2, Fe2B, Fe3Si, α-Fe, Fe-B composite and a residual amorphous phase.

AB - The magnetic order and crystallization of the amorphous Fe 75Si15B10 alloy prepared by mechanical alloying was studied in situ by 57Fe Mössbauer spectroscopy. These measurements were carried out using a vacuum furnace, controlling the temperature in the absorber. From Mössbauer measurements the magnetic order temperature of the as-milled sample was estimated at about 675 K. In order to identify the crystalline phases formed during heating, Mössbauer measurements were analyzed together with X-ray diffraction analysis. Both results show the formation of several crystalline phases such as Fe 5SiB2, Fe2B, Fe3Si, α-Fe, Fe-B composite and a residual amorphous phase.

KW - Mechanical alloying

KW - Metallic alloys

KW - Mössbauer spectroscopy

KW - Soft magnetic materials

UR - http://www.scopus.com/inward/record.url?scp=0347063895&partnerID=8YFLogxK

U2 - 10.1023/B:HYPE.0000003769.28718.19

DO - 10.1023/B:HYPE.0000003769.28718.19

M3 - Artículo

AN - SCOPUS:0347063895

SN - 0304-3843

VL - 148-149

SP - 97

EP - 102

JO - Hyperfine Interactions

JF - Hyperfine Interactions

IS - 1-4